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Acidic aqueous work up and purification by silica gel column chromatography using a ethyl acetate EtOAc hexan gradient EtOAc hexane 1 4, v v EtOAc hexane 3 7, v v afforded 207 mg g 65 yield of the target compound 56a as a viscous oil priligy BMJ 346, f4116 2013
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Acidic aqueous work up and purification by silica gel column chromatography using a ethyl acetate EtOAc hexan gradient EtOAc hexane 1 4, v v EtOAc hexane 3 7, v v afforded 207 mg g 65 yield of the target compound 56a as a viscous oil priligy BMJ 346, f4116 2013
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